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目 录 第一章. 预启动检查 ........................................................................................... 10 1-1. 硬件 ............................................................................................................. 10 1-2. 实验调度文件（实验过程文件）.............................................................. 10 1-3. 恒电位仪模式&循环器模式 ...................................................................... 10 1-4. 虚拟控制面板 ............................................................................................. 11 1-5. 校准 ............................................................................................................. 11 第二章. 一般性说明 ........................................................................................... 12 2-1. 安装 ............................................................................................................. 12 2-1-1 硬件安装 .................................................................................................. 12 2-1-2. 软件安装 ................................................................................................. 12 2-2. 检查点 ......................................................................................................... 15 2-3. 注意事项 ..................................................................................................... 16 2-4. 前面板 ......................................................................................................... 17 2-5. 后面板 ......................................................................................................... 19 第三章. 文件菜单 ............................................................................................... 20 3-1. 打开实验条件文件 ..................................................................................... 20 3-2. 普通数据文件的ASCII文件转换 ............................................................... 24 3-3. 循环数据文件和容量数据文件的ASCII转换 ............................................ 22 3-4. 分割普通数据文件 ...................................................................................... 22 3-5. ASCII文件到二进制文件转换 .................................................................... 22 第四章. 实验菜单 ................................................................................................ 23 4-1. 电分析技术 .................................................................................................. 24 4-1-1 循环伏安法 ................................................................................................ 24 4-1-2 线性扫描伏安法 ........................................................................................ 26 4-1-3 计时安培法 ................................................................................................ 27 4-1-4 计时库仑法 ................................................................................................ 28 4-1-5 计时电位法 ................................................................................................ 29 4-1-6 方波伏安法-选配 ....................................................................................... 30 4-1-7 溶出模式–选配 ......................................................................................... 32 4-2. 直流腐蚀测量 ................................................................................................ 36 4-2-1 Tafel图 ......................................................................................................... 36 4-2-2 动态电位 ...................................................................................................... 38 4-2-3 静态电位 ...................................................................................................... 40 4-2-4 动态电流 ...................................................................................................... 42 4-2-5 静态电流 ...................................................................................................... 45 4-2-6 循环极化 ...................................................................................................... 46 4-2-7 Ecorr vs. 时间 .............................................................................................. 48 4-2-8 线性极化电阻 ............................................................................................... 49 4-2-9 Rp/Ec趋势-选配 ........................................................................................... 51 4-2-10 电偶腐蚀-选配 ............................................................................................ 53 4-3. 实验调度文件的创建 ...................................................................................... 55 4-3-1 测试信息 ........................................................................................................ 56 4-3-2 创建实验调度文件 ........................................................................................ 57 第五章 控制菜单 ..................................................................................................... 62 5-1. 监测和控制 ...................................................................................................... 62 第六章 图形菜单 ..................................................................................................... 67 6-1 基本图形功能 ................................................................................................... 68 6-1-1 用户标度 ....................................................................................................... 68 6-1-2 放大功能 ....................................................................................................... 68 6-1-3 图形网格 ....................................................................................................... 68 6-1-4 坐标值读取 .................................................................................................. 69 6-1-5 斜率计算 ..................................................................................................... 69 6-1-6 文本插入 ..................................................................................................... 70 6-1-7 ASCII转换 .................................................................................................... 70 6-1-8 复制到剪贴板 .............................................................................................. 71 6-1-9 图形格式设置 .............................................................................................. 71 6-2. 普通数据图形 ................................................................................................. 71 6-2-1 坐标轴参数 .................................................................................................. 72 6-2-2 普通数据图形的特殊绘图 .......................................................................... 74 1）仅充电图形 ....................................................................................................... 74 2）仅放电图形：同上，除了按钮不一样（红色）............................................. 75 3）充电和放电图形：+ & - 按钮按下 ................................................................... 75 4）示例 .................................................................................................................... 76 6-3 循环数据图形 .................................................................................................. 78 6-3-1 坐标轴参数 .................................................................................................. 78 6-4 阶跃数据图形 .................................................................................................. 79 第七章 报告 ............................................................................................................. 80 7-1. 循环条件文件报告 .......................................................................................... 80 7-2. 循环数据报告 ................................................................................................. 81 7-3. 容量数据报告 ................................................................................................. 82 7-4. 阶跃数据报告 ................................................................................................. 82 7-5. 校准数据报告 ................................................................................................. 83 附录 ......................................................................................................................... 84 附录1. 电解池连接 ................................................................................................ 84 A1-1 电池测试 ........................................................................................................ 84 A1-2 电化学实验和半电池测试 ............................................................................ 85 A1-3. 电偶腐蚀测试 ............................................................................................... 85 附录2. 校准 ............................................................................................................. 86 A2-1 使用外部电阻 ................................................................................................ 86 A2-2 使用简单校准套件（选配）.......................................................................... 87 A2-3 使用模拟电解池（选配）.............................................................................. 88 A2-4. 校准程序：xcalib.exe .................................................................................. 89 附录3. 工具条 .......................................................................................................... 91 附录4. 电池测试菜单-选配 ..................................................................................... 92 A4-1 里电池测试菜单 ............................................................................................. 92 A4-2 NiCd（NiMH）电池测试菜单 ...................................................................... 93 附录5. 导线和通讯模块 .......................................................................................... 94 A5-1. 电解池导线 .................................................................................................... 94 A5-3. 通讯模块 ........................................................................................................ 95