中文版用户手册
目录 第一章. 预启动检查........................................................................................ 11 1-1.硬件........................................................................................................... 11 1-2. 实验调度文件(实验过程文件)...........................................................11 1-3. 恒电位仪模式 & 循环器模式................................................................ 11 1-4. 虚拟控制面板.......................................................................................... 12 1-5. 校准.......................................................................................................... 12 第二章. 一般性说明.........................................................................................13 2-1. 安装.......................................................................................................... 13 2-2. 检查点...................................................................................................... 13 2-3. 注意事项 ..................................................................................................15 第三章. 文件菜单............................................................................................16 3-1. 实验调度文件的创建...............................................................................16 3-1-1 测试信息.................................................................................................18 3-1-2 创建实验调度文件.................................................................................19 3-2. 打开/编辑实验调度文件..........................................................................26 3-3. 普通数据文件的ASCII文件转换.............................................................26 3-4. 循环数据文件,阶跃数据文件 & 容量数据文件的ASCII转换 ...........28 3-5. 分割普通数据文件....................................................................................28 3-6. ASCII文件到二进制文件的转换 .............................................................29 3-7. 图形打印选项............................................................................................30 第四章. 实验菜单-选项 ...................................................................................31 4-1. 电分析技术................................................................................................32 4-1-1 循环伏安法..............................................................................................32 4-1-2 线性扫描伏安法......................................................................................34 4-1-3 计时电流法..............................................................................................36 4-1-4 计时库仑法..............................................................................................38 4-1-5 计时电位法 .............................................................................................40 4-1-6 方波伏安法 –选项............................................................................... 42 4-1-7 溶出模式 –选项................................................................................... 44 4-2. 直流腐蚀测量............................................................................................ 48 4-2-1 Tafel图.....................................................................................................48 4-2-2 动态电位.................................................................................................. 50 4-2-3 静态电位.................................................................................................. 52 4-2-4 动态电流.................................................................................................. 54 4-2-5 静态电流.................................................................................................. 56 4-2-6 循环极化.................................................................................................. 58 4-2-7 Ecorr vs. 时间 ..........................................................................................60 4-2-8 线性极化电阻 ...........................................................................................62 4-2-9 Rp/Ec趋势(选项) ................................................................................64 4-2-10 电偶腐蚀(选项) .................................................................................66 第五章. 控制菜单 ...............................................................................................68 5-1. 监测 & 控制 ................................................................................................68 5-1-1. 实验过程 ..................................................................................................69 5-1-2 单通道操作 ...............................................................................................70 5-1-3 多通道操作 ...............................................................................................72 5-1-4 停止预设 ...................................................................................................73 5-2. 监测 ..............................................................................................................75 5-2-1 长图图形 ....................................................................................................75 5-2-2 简易监测器 ................................................................................................76 5-2-3 详细监测器 ................................................................................................77 5-2-4 软件UPS功能. ...........................................................................................78 第六章. 图形菜单 .................................................................................................80 6-1 基本图形功能 ................................................................................................81 6-1-1 用户标度 .....................................................................................................81 6-1-2 放大功能 .....................................................................................................81 6-1-3 图形网格 .....................................................................................................81 6-1-4 坐标值读取 .................................................................................................82 6-1-5 斜率计算 .....................................................................................................82 6-1-6 文本插入 .....................................................................................................83 6-1-7 ASCII转换 ...................................................................................................83 6-1-8 复制到剪贴板 .............................................................................................83 6-1-9. 图形格式设置 ............................................................................................84 6-2. 普通数据图形 ................................................................................................85 6-2-1 坐标轴参数 ..................................................................................................85 6-2-2 普通数据图形的特殊绘图 ..........................................................................87 1) 仅充电图形 ........................................................................................................87 2) 仅放电图形:同上,除了按钮图标不一样(红色) ....................................87 3) 充电 & 放电图形:+ & - 图标按下. ................................................................88 4) 示例 ....................................................................................................................89 6-3 循环数据图形 ..................................................................................................90 6-3-1 坐标轴参数 ..................................................................................................90 6-4 阶跃数据图形 ..................................................................................................91 第七章. 报告 ...........................................................................................................92 7-1. 实验调度文件报告 ..........................................................................................92 7-2. 普通数据报告 ..................................................................................................93 7-3. 循环数据报告 ..................................................................................................94 7-4. 容量数据报告 ..................................................................................................94 7-5. 阶跃数据报告 ..................................................................................................95 7-6. 校准数据报告 ..................................................................................................95 第八章. 备份 ...........................................................................................................96 附录 附录 1. 电解池连接 ................................................................................................97 A1-1. 电池测试 ........................................................................................................97 A1-2. 普通电化学 ....................................................................................................98 A1-3. ZRA(零阻计)测试 –选项 .......................................................................99 附录 2. 通道校准 .....................................................................................................100 A2-1. 利用用户的外部电阻 .....................................................................................100 A2-2 利用简易校准套件(选配件) ......................................................................102 A2-3 利用模拟电解池(选配件) ..........................................................................103 A2-4. 校准程序:xcalib.exe ....................................................................................104 附录 3. 工具条 ..........................................................................................................106 附录 4. 电池测试菜单 –选项 ................................................................................107 A4-1 锂电池测试菜单 ...............................................................................................107 A4-2 NiCd(NiMH)电池测试菜单 .............................................................................108 附录 5. 模块 & 附件 ................................................................................................109 A5-1 PGPIM通道模块(标准型) ............................................................................109 A5-2 AuxV辅助电压模块 –选配件 ..........................................................................110 A5-3. 温度测量模块(选配件) ................................................................................111 A5-4. 电解池线缆 .........................................................................................................112 附录 6. 界面线缆连接 .................................................................................................113 A6-1 界面线缆(PC-仪器) .......................................................................................114 A6-2. 界面线缆互连(仪器-仪器) ............................................................................115 A6-3. 界面卡 ..................................................................................................................116 A6-4 连接向导 ...............................................................................................................117 附录 7. 操作提示 ..........................................................................................................118 附录 8. 安全限制 & 故障功能 .....................................................................................131